Epa method 6010c pdf

Selected analytical methods for environmental remediation and recovery sam 2017. As with other usepa mandated methods, 6010c requires adherence to specific procedures to ensure analytical quality. Method 6010c is the fourth version of this method and was released as part of sw846 update iv. Inductively coupled plasmaatomic emission spectrometry summary. Fast sample throughput and low cost analysis is desirable for these labs but can be challenging to achieve using spectrochemical techniques due to the wide range of elements and their varying concentrations in typical samples. Since sample preparation method 3050b cannot provide for an analysis of mercury, when you prepare a sample for analysis of mercury you must use the sample preparation method established for analysis method 7470a when using method 7470a to analyze your sample and the sample preparation method established for analysis method 7471a when using method 7471a to analyze your product. Method 6010c l ess than 10% of analyte level of sample or less than 10% of regulatory limit. It is usually best to use the most updated version due to rapidly changing technology. Deviations from tests and calibration methods shall occur only if the deviation has been documented, technically justified, authorized, and accepted. The instrument measures characteristic emission spectra by optical spectrometry. Samples are nebulized and the resulting aerosol is transported to the plasma torch. The method has gone through a series of updatesfrom epa 6010, 6010a, 6010b, 6010c, and in july 2014, to 6010d update v.

Analysts should consult the disclaimer statement at the front of the manual and. Epa 8280, cadhsluft7420 if it is not aqueous and, when mixed with an equivalent weight of water, produces a solution having a ph. Inductively coupled plasmaoptical emission spectrometry icpaes the following document details the method used to describe multielemental determinations by icpaes using sequential or simultaneous optical systems and axial or radial viewing of the plasma. View actual epa method 6010c pdf file epa method 6010c. This document is included in selected analytical methods for environmental remediation and recovery sam. Us epa sw846 method 6010d using the icap 7400 icpoes duo. This method describes multielemental determinations by icpaes using sequential or simultaneous optical systems and axial or radial viewing of the plasma. This application note describes the performance of the thermo scientific icap 7400 icpoes duo for the analysis of environmental sample types by the us epa method 6010d. Epas selected analytical methods for environmental remediation and recovery sam lists this method for analysis of solid, non drinking water. Methods for the chemical analysis of water and wastes mcaww epa 600479020 citation information.

Environmental protection agency, washington, dc, epa600r17356, 2017. Many laboratories quantify elements in environmental samples, such as industrial wastes, soils, sludge and sediment by icpoes. The information contained in this method is provided by epa as guidance to be. Ground water site that was analyzed for the following parameters and u. The information contained in this method is provided by epa as guidance to be used. Sediments, sludges, and soils or us epa method 3051a microwave assisted digestion of sediments, sludges, soils and oils. An43152 e 01c us epa sw846 method 6010c using the thermo. Environmental sampling and analytical methods esam program. Methods for the determination of metals in environmental. Sw846 is not intended to be an analytical training manual. Us epa method 6010c is used within the usa and its variants are widely used in other regions, therefore the ability to undertake this type of analysis using us epa method 6010c represents an important. Inductively coupled plasmaatomic emission spectrometry icpaes may be used to determine trace elements in solution. High throughput, low cost icpoes analysis of sludge samples. As indicated in the method, all samples other than filtered, preserved groundwaters require acid digestion prior to analysis.

This method is applicable to ground waters, tclp and extraction procedure ep toxicity extracts, industrial organic wastes, soils, sludge, and sediments. The following is a listing of analytical methods commonly utilized by contest analytical laboratory. Selected analytical methods for environmental remediation and. Epa methods and guidance for analysis of water, version 2. The method is simple, rapid, and applicable to a large number of metals in drinking, surface, and saline waters and domestic and industrial wastes. Prior to analysis, samples must be solubilized or digested using the appropriate sample preparation methods. A list of methods in the 6000 series with links to more detailed documents that summarize application and scope. All of the documents found in the third edition of sw846, as updated by updates i, ii, iia, iib, iii, iiia, iiib, iva and ivb are located at this site. Dispersion icp for performing analysis according to sw846 method 6010c. United states environmental protection agency region 9. Can digests from those two methods be used directly on an automated mercury analyzer without any further sample treatment elimination. Therefore, method procedures are written based on the assumption that they will be performed by analysts who are. The information contained in this method is provided by epa as guidance to be used by the analyst and the regulated community in making judgments necessary to generate results that meet the dqos for the intended application. The method is applicable to all of the elements listed in table 1.

Epa will correct these errors in the next revision of the method. Soil metals analysis by icpoes icpoes analysis of trace metals in soils, sludges and sediments. Epa sw846 method 6010c using the prodigy7 highdispersion icp introduction application note an5 an5 usepa sw846 method 6010c prodigy7. Determination of lead in tsp by inductively coupled. Environmental protection agency usepa under epa contract no.

One of the specified methods is us environmental protection agency epa method. Us epa sw846 method 6010d using the icap 7400 icpoes duo author. As indicated by the epa, the analytical methods in sw846. Analyzing trace elements with epa method 6010 thermo fisher.

Dwmicrowave digestionheating allowed by epa maintaining method heating temperatures in referenced method. When analyzing groundwater samples for dissolved constituents, acid digestion is not necessary if the samples are. Pdf icon view actual epa method 6010c pdf file epa method 6010c. Dallas wait, chair environmental laboratory advisory. This method is for analysis of 21 trace metal elements in drinking, surface, and ground waters, and can also be used for solid waste samples. Sw846 contains over 200 documents, including the table of contents, disclaimer, preface, chapters one through thirteen, and many different methods for the sampling and analysis of wastes. Letter from elab to the forum on environmental measurements. Inductively coupled plasmaatomic emission spectrometry, revision 4. The laboratory is responsible for maintaining a safe work environment and a current awareness file of osha regulations regarding the safe handling of the chemicals specified in this method. As noted in our june 30, 2016 letter, the fem membership shared elabs letter with key individuals to further discuss method harmonization across the agency. United states environmental protection agency region 9 laboratory 37 s. Mercury is listed as an analyte in both draft update iva method 3015a and method 3051a.